In situ mechanical compression of polycrystalline BaTiO3 in the ESEM

Angelika Reichmann; Stefan Mitsche; Armin Zankel; Peter Pölt; Klaus Reichmann

doi:10.1016/j.jeurceramsoc.2014.03.015

In situ mechanical compression of polycrystalline BaTiO3 in the ESEM

Angelika Reichmann^*, Stefan Mitsche, Armin Zankel, Peter Pölt, Klaus Reichmann

^*Corresponding author for this work

Research output: Contribution to journal › Article › peer-review

Abstract

Ferroelectric BaTiO3 was mechanically compressed in situ, in an environmental scanning electron microscope equipped with a compression stage and domain wall motion was recorded using orientation contrast imaging. Before and after the experiment, the sample was characterized by electron backscatter diffraction (EBSD) in order to determine the misorientation between single domains which was 90° in every case. During the compression test, the microstructure changed from a banded twin structure to lamellar twinning

Original language	English
Pages (from-to)	2211-2215
Journal	Journal of the European Ceramic Society
Volume	34
Issue number	10
DOIs	https://doi.org/10.1016/j.jeurceramsoc.2014.03.015
Publication status	Published - 2014

Fields of Expertise

Advanced Materials Science

Treatment code (Nähere Zuordnung)

Experimental

Access to Document

10.1016/j.jeurceramsoc.2014.03.015

In-situ Experiments in the ESEM
Zankel, A., Pölt, P. & Reingruber, H.
1/01/09 → 31/12/23
Project: Research project
CD-Laboratory for Advanced Ferroic Oxides
Reichmann, K.
1/01/08 → 31/12/14
Project: Research project

Cite this

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title = "In situ mechanical compression of polycrystalline BaTiO3 in the ESEM",

abstract = "Ferroelectric BaTiO3 was mechanically compressed in situ, in an environmental scanning electron microscope equipped with a compression stage and domain wall motion was recorded using orientation contrast imaging. Before and after the experiment, the sample was characterized by electron backscatter diffraction (EBSD) in order to determine the misorientation between single domains which was 90° in every case. During the compression test, the microstructure changed from a banded twin structure to lamellar twinning",

author = "Angelika Reichmann and Stefan Mitsche and Armin Zankel and Peter P{\"o}lt and Klaus Reichmann",

year = "2014",

doi = "10.1016/j.jeurceramsoc.2014.03.015",

language = "English",

volume = "34",

pages = "2211--2215",

journal = "Journal of the European Ceramic Society",

issn = "0955-2219",

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T1 - In situ mechanical compression of polycrystalline BaTiO3 in the ESEM

AU - Reichmann, Angelika

AU - Mitsche, Stefan

AU - Zankel, Armin

AU - Pölt, Peter

AU - Reichmann, Klaus

PY - 2014

Y1 - 2014

N2 - Ferroelectric BaTiO3 was mechanically compressed in situ, in an environmental scanning electron microscope equipped with a compression stage and domain wall motion was recorded using orientation contrast imaging. Before and after the experiment, the sample was characterized by electron backscatter diffraction (EBSD) in order to determine the misorientation between single domains which was 90° in every case. During the compression test, the microstructure changed from a banded twin structure to lamellar twinning

AB - Ferroelectric BaTiO3 was mechanically compressed in situ, in an environmental scanning electron microscope equipped with a compression stage and domain wall motion was recorded using orientation contrast imaging. Before and after the experiment, the sample was characterized by electron backscatter diffraction (EBSD) in order to determine the misorientation between single domains which was 90° in every case. During the compression test, the microstructure changed from a banded twin structure to lamellar twinning

U2 - 10.1016/j.jeurceramsoc.2014.03.015

DO - 10.1016/j.jeurceramsoc.2014.03.015

M3 - Article

SN - 0955-2219

VL - 34

SP - 2211

EP - 2215

JO - Journal of the European Ceramic Society

JF - Journal of the European Ceramic Society

IS - 10

ER -

In situ mechanical compression of polycrystalline BaTiO3 in the ESEM

Abstract

Fields of Expertise

Treatment code (Nähere Zuordnung)

Access to Document

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Projects

In-situ Experiments in the ESEM

CD-Laboratory for Advanced Ferroic Oxides

Cite this