Projects per year
Temperature modulated thermophysical measurements can deliver valuable insights into the phase transformation behavior of many different materials. While especially for non-metallic systems at low temperatures numerous powerful methods exist, no high-temperature device suitable for modulated measurements of bulk metallic alloy samples is available for routine use. In this work a dilatometer for temperature modulated isothermal and non-isothermal measurements in the temperature range from room temperature to 1300 K is presented. The length measuring system is based on a two-beam Michelson laser interferometer with an incremental resolution of 20 pm. The non-contact measurement principle allows for resolving sinusoidal length change signals with amplitudes in the sub-500 nm range and physically decouples the length measuring system from the temperature modulation and heating control. To demonstrate the low-amplitude capabilities, results for the thermal expansion of nickel for two different modulation frequencies are presented. These results prove that the novel method can be used to routinely resolve length-change signals of metallic samples with temperature amplitudes well below 1 K. This high resolution in combination with the non-contact measurement principle significantly extends the application range of modulated dilatometry towards high-stability phase transformation measurements on complex alloys.
|Journal||Review of Scientific Instruments|
|Publication status||Published - 2016|
Fields of Expertise
- Advanced Materials Science
FingerprintDive into the research topics of 'A high-stability non-contact dilatometer for low-amplitude temperature-modulated measurements'. Together they form a unique fingerprint.
- 2 Active
Defects & Transformations of Materials
Klinser, G., Sprengel, W. & Würschum, R.
1/01/13 → …
Project: Research area
Atomic defects in metals and metals oxides
Sprengel, W., Würschum, R., Klinser, G. & Resch, L.
1/01/12 → …
Project: Research project