Simulation and Experiment of the Homogeneously Catalyzed Production of Terpenyl Amine

Robin Schulz, Laura Sengen, Katja Gießelmann, Sira Hunold, Tim Zeiner

Publikation: Beitrag in einer FachzeitschriftArtikelForschungBegutachtung

Abstract

Continuous terpenyl amine production via a homogeneously catalyzed hydroamination is presented. For the recycling of the catalyst a liquid-liquid system combined with a subsequent acid complexation as capturing step for the terpenyl amine was used. The whole process was run in pilot plant scale. At first, batch experiments were conducted to determine reaction equilibria of the hydroamination and the acid complexation. On this, a process model was developed which is based on equilibrium stages. This process model was validated by running the continuous process and was able to predict the continuous process in good agreement with experimental data. So, it allows a reduction of the experimental effort.

Originalspracheenglisch
Seiten (von - bis)947-955
Seitenumfang9
FachzeitschriftChemie - Ingenieur - Technik
Jahrgang90
Ausgabenummer7
DOIs
PublikationsstatusVeröffentlicht - 1 Jul 2018

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Complexation
Amines
Acids
Liquids
Pilot plants
Recycling
Experiments
Catalysts

Schlagwörter

    ASJC Scopus subject areas

    • !!Chemistry(all)
    • !!Chemical Engineering(all)
    • !!Industrial and Manufacturing Engineering

    Dies zitieren

    Simulation and Experiment of the Homogeneously Catalyzed Production of Terpenyl Amine. / Schulz, Robin; Sengen, Laura; Gießelmann, Katja; Hunold, Sira; Zeiner, Tim.

    in: Chemie - Ingenieur - Technik, Jahrgang 90, Nr. 7, 01.07.2018, S. 947-955.

    Publikation: Beitrag in einer FachzeitschriftArtikelForschungBegutachtung

    Schulz, Robin ; Sengen, Laura ; Gießelmann, Katja ; Hunold, Sira ; Zeiner, Tim. / Simulation and Experiment of the Homogeneously Catalyzed Production of Terpenyl Amine. in: Chemie - Ingenieur - Technik. 2018 ; Jahrgang 90, Nr. 7. S. 947-955.
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